We then added 10cm3 ethanoic anhydride to the salicylic acid and swirled the contents, this mixes together the two chemicals. We then added 5 drops of concentrated sulphuric acid to the flask and thoroughly swirled the mixture, this creates the solution that makes the aspirin. We then warmed the flask for 20 minutes in a 400cm3 beaker of hot water which was approximately 60°C, we made sure the flask did not go above 65°C because this could have caused the contents to evaporate. Part 2: Using a 25cm3 measuring cylinder we measured out 15cm3 of ethanol into a boiling tube and then prepared a beaker half filled with hot water at approx. 75°C, we got this temperature by filling the beaker with cold water and slowly adding boiling water from a kettle until we reached the right temperature.
when the pH is 7, allow the solution to cool to room temperature. f. Add about 50 ml water to the solution and stir it. Filter the pale blue precipitate in a Buchner funnel.it is observed that the mixture filters slowly, the way to solve the little problem is to stir the precipitate with 50 ml more water. Wash the precipitate with water followed with alcohol. Place the mixture in a petri dish and let it dry in an oven at 140 ˚C for six hours.
We added sodium carbonate until the pH of the mixture was 8. After neutralize, we collected benzocaine by vacuum filtration. We used a Buchner funnel to collect benzocaine. We used three 10 ml of water to wash the product. After the product was dry, we weighed, calculate the percent yield and determined the melting point of the product.
The crude tetraphenylnaphthalene in a 25-ml Erlenmeyer flask and dissolved in boiling isopropyl alcohol (12 ml). The solution was cooled to room temperature and further cooled in an ice bath for 30 minutes. Crystallization of colorless crystals occurred. The product was collect in a Hirsch funnel and washed with isopropyl alcohol. The solid was left to dry over the weekend.
The tube was placed back in incubation for 96 more hours to observe any more positives. 2.10 Catalase Test A trypticase soy agar plate was used and after incubation, four drops of 3% Hydrogen Peroxide was added to the plate to flow over the bacterial growth. A presence of bubbling was observed. 2.11 Starch Hydrolysis A starch agar plate was inoculated with a streak of the unknown bacteria and then incubated. On the second day of incubation, the plate was removed from the incubator and placed over a hot plate heating Iodine solids.
Then an estimated (by trial and error) 1-3 grams of hydrated copper sulfate was added to a crucible with the lid on top. The total mass of the hydrated copper sulfate was recorded by subtracting the total mass of the crucible, lid, and sample from the mass of the crucible and lid (described in table 1.3). By attaching the wire triangle to the ring, the crucible was able to sit securely while having the bunsen burner underneath. Lighting the burner once again, each substance was heated for several minutes until estimated that the compound had changed color. Once a prevalent color change had been observed at approximately 4 minutes (blue green color) the crucible was set on the counter using the tongs to cool for approximately 5 minutes.
Put 1 capsule of the bioflorin into each of the test tubes and tap them until the capsule dissolves. Screw the liquid onto both test tubes to make sure that they are sealed. You now have to wait for approximately two days, in order to obtain satisfying results. Light the candle/put it on fire. Fill the third test tube with approximately two millimeters of Ethanol.
7. Bake at 400 F for 30-40 minutes or until golden. 8. Remove from the pan and let completely cool for about 2 hours. Cuisine: American Course: Lunch, Breakfast Recipe Notes When measuring flour, use a dry measuring cup and a straight edge to level the flour.
For the orange sauce: In a medium sauce pan, bring to a boil 250 ml (8.5 fluid ounces) of water and orange zest. Simmer for 5 more minutes. Strain, add sugar and lemon juice bring back to a simmer. Dissolve corn starch in the remaining 50 ml of water. Very slowly, pour it into a simmering mixture of water and juice, whisking
Water was removed from the dish, and the Cu was then washed thrice with 5 mL deionized water, and decanted between washings. It was then similarly washed thrice with 5 mL of ethanol. The evaporating dish was then placed on the steam bath to dry until the Cu had a sand-like texture. The bottom of the dish was dried, it was cooled to room temperature, and then its mass was measured and recorded. All the solutions were disposed of in the liquid waste container, the Cu and Al were disposed of in the solid waste container, and the apparatus was cleaned and put