1. In part A. organic compounds benzophenone was mixed with water after 60 seconds it was determined the compound was insoluble in water. Similarly, to water it was found that hexane which in non polar was semi soluble. The only soluble solvent was methyl alcohol which was detected after 20 seconds. When determining the solubility of malonic acid in different solvents both water and methyl alcohol were found to be polar when mixed with malonic acid. Hexane however was insoluble. Lastly biphenyl was mixed with water and was found to be insoluble, methyl alcohol was determined to be partially soluble.Hexane on the other hand was the only soluble solvent for biphenyl 2. Part B. of this experiment determined the solubility of different alcohols in hexane or water. Alcohols 1-Octanol, and 1-butanol were both found to be soluble in hexane while methyl alcohol was determined to be insoluble. when water was added to the different alcohols the opposite reaction occurred compared to hexane. 1-Octanol, and 1-butanol were both insoluble while methyl alcohol was the only soluble alcohol. 3. …show more content…
In part C. pairs of compounds were investigated to determine whether the compounds were miscible or immiscible. Diethyl ether and methylene chloride, diethyl ether and ethyl alcohol, water and ethyl alcohol, heptane and methyl chloride, and heptane and diethyl ether were all were found to be miscible each of these paired compounds showed a homogenous mixture with no chunks or particles left over when combined. On the other hand, water and heptane, water and methylene chloride, and water and diethyl ether were all immiscible, when mixed together it was observed that the compounds had two layers rather than one homogenous
The goal of this experiment was to isolate three different molecules (acidic, basic, and neutral) from a mixture and identify their molecular structure. This was accomplished by using acid/base liquid extraction and H NMR analysis. The neutral component of the unknown mixture #191 was fluorenone. This was evident due to an H NMR spectra that had a high presence of hydrogen signals in the 7.2- 7.7 ppm range. Chemical shift values for fluorenone stated in the lab manual were 7.27, 7.47, 7.48, and 7.6 (CITE), indicating that the corresponding H NMR spectra for the neutral unknown is of this chemical.
Since it is also a solvent, it has many cleaning uses. We predicted at once that is could be isopropanol because of its smell. Question: “What is the identity of unknown 6 in test tube 20?” Hypothesis: If I test the characteristic properties of unknown 6 then I will see its properties to be the same or similar to isopropanol.
To begin, the solubility of the unknown compound in water was tested. If the compound is soluble in water, it can be inferred that it is either a polar covalent or ionic compound.
Molecular Structure Lab Report: Determining Polarity Instructions: For this investigative phenomenon, you will investigate why certain substances, such as oil and vinegar, don't mix. To do so, you will combine various compounds, compare their solubility, and determine their polarity. Fill in each section of this lab report and submit it to your instructor for grading.
The goal of the experiment is to synthesize a bromohexane compound from 1-hexene and HBr(aq) under reflux conditions and use the silver nitrate and sodium iodide tests to determine if the product is a primary or secondary hydrocarbon. The heterogeneous reaction mixture contains 1-hexene, 48% HBr(aq), and tetrabutylammonium bromide and was heated to under reflux conditions. Heating under reflux means that the reaction mixture is heated at its boiling point so that the reaction can proceed at a faster rate. The attached reflux condenser allows volatile substances to return to the reaction flask so that no material is lost. Since alkenes are immiscible with concentrated HBr, tetrabutylammonium bromide is used as a phase-transfer catalyst.
Unknown compounds verification Introduction: In Project 3 we are going to test an unknown compound and there are several different ways that can help us to identify the Unknown substance. And there is some pre-lab information that found in the internet. By Experiment 3: Identification of a Substance by Physical Properties “Every substance has a unique set of properties that allow us to differentiate one from another. These properties can be classified as either physical properties or chemical properties.
After obtaining an homogeneous mixture, the flask was placed in an ice bath during five minutes next to a graduated cylinder containing 5.0 mL of concentrated sulfuric acid. The temperature of the ice bath was recorded to be 1.1 °C. Likewise, a second graduated cylinder containing 1.8 mL of nitric acid and 2.5 mL of sulfuric acid was immersed in the cold ice bath to keep the three different solutions at the same temperature. Thereafter, the cold 5.0 mL of H2SO4 were added to the erlenmeyer flask containing the acetanilide solution, which remained in the cold water for approximately another 4 minutes.
The membrane permeability of Beta vulgaris is affected by ethanol solution Introduction Cell membranes are the semi-permeable membrane that surrounds all cells. It separates the extracellular environment from the intercellular environment. It is a phospholipid bilayer which contains various proteins, lipids and carbohydrates all serving different purposes. It is this structure which allows for the transport of nutrients, proteins and water. (Nature.com, 2014).
In the round-bottom flask (100 mL), we placed p-aminobenzoic acid (1.2 g) and ethanol (12 mL). We swirled the mixture until the solid dissolved completely. We used Pasteur pipet to add concentrated sulfuric acid (1.0 mL) to the flask. We added boiling stone and assembled the reflux. Then, we did reflux for 75 minutes.
Elijah Brycth B. Jarlos IX-Argon 1. Multicellularity is a condition of an organism to have multicellular cells. An example of a organism who has multicellular cells are plants, animals, and humans. The main reason of why scientists have a hard time finding a good set of existing organisms to compare. Is neither the first set of organisms which is being compared is dying as fast as the second specimen is being examined or they just can’t find the right species.
In this lab, we tested 8 known ingredients to find what ingredients was in our unknown A and unknown B medications. We first tested the water solubility of our knowns and unknowns. We found that of the knowns, cornstarch and acetaminophen were the only ones not water soluble. The unknowns were also not water soluble. Th next test was the pH test.
Next, a 100 mL graduated cylinder was used to measure 60 mL of distilled water. The water was added to the compound and stirred with a glass-stirring rod until dissolved. Next, The flame test required the solution made during the solubility test. The experiment needed a metal wire that was dipped into the solution
.048 1.0 94.1 Experiment Two Methanol (MeOH) And Water (H2O) .049 .045 Methanol – 1.5 Water – 0.5 92 Conclusion Both experiments were of fair solubility, but in the case of recrystallization of Benzoic Acid, Water was the best solvent to recrystallize acid the most. Experimental data determined that there was a difference of .003g between using the single solvent in comparison to the paired solvent.
This method which uses an internal standard and flame ionisation detector, is exact and more specific than methods usually used. The gas-liquid chromatography method determines ethanol clearly and separately from the other beverage components that would have interfered in other methods, without any distillation or need for a chemical reaction. Determination of ethanol is one of the most vital routine analysis in a current winery. This method provides frequent, rapid and accurate results are needed to regulate the quality of the wine from grape to bottle, as well as for state and federal government
It was calculated and found that the concentration of benzoic acid was higher at 30℃ (0.0308M) than at 20℃