Method A) Prepare a NaOH solution (approximately 0,1M NaOH) 1. Place a clean, dry glass beaker on the electronic scale. 2. Determine the mass of the glass beaker. 3. Tare the scale. 4. Measure out 2g of NaOH pellets into the glass beaker. 5. Determine the mass of the beaker and NaOH together. 6. Rinse a 500 ml volumetric flask with deionized water. 7. Label the volumetric flask so you know which solution is in it. 8. Place a clean funnel into the mouth of a 500ml volumetric flask. 9. Carefully pour the NaOH pellets into the funnel. 10. Use the wash bottle with deionised water to transfer all the NaOH pellets from the glass beaker to the funnel. 11. Rinse out all the NaOH pellets with the wash bottle from the funnel in the volumetric flask. …show more content…
Swirl the solution to ensure that the NaOH is properly dissolved in the deionised water. B) Prepare an Oxalic Acid Solution (approximately 0,05M) 1. Place a clean, dry glass beaker on the electronic scale. 2. Determine the mass of the glass beaker. 3. Tare the scale. 4. Measure out 1,575g of oxalic acid crystals into the glass beaker. 5. Determine the mass of the beaker and NaOH together. 6. Rinse a 250 ml volumetric flask with deionized water. 7. Label the volumetric flask so you know which solution is in it. 8. Place a clean funnel into the mouth of a 250ml volumetric flask. 9. Carefully pour the oxalic acid crystals into the funnel. 10. Use the wash bottle with deionised water to transfer all the oxalic acid crystals from the glass beaker to the funnel. 11. Rinse out all the oxalic acid crystals with the wash bottle from the funnel in the volumetric flask. 12. Add deionized water to the volumetric flask to the 250ml mark on the volumetric flask. 13. Read the volume from the bottom of the meniscus. 14. Swirl the solution to ensure that the oxalic acid crystals are properly dissolved in the deionised water. C) Measuring pH of HCl Solution (unknown Concentration) with an indicator 1. Pour 20 ml of HCl into a
A hot plate was placed under the ring stand. 50 mL of 3.0 M NaOH in a 250 mL beaker and a stir bar was placed in the beaker. The beaker with NaOH was placed on the hot plate and 3.75 grams of NaAlO2*5H2O was placed in the beaker. The temperature probe was placed in the beaker with the solution, not touching the bottom of the beaker. The solution was heated and stirred till the solution dissolved.
To begin this, experiment our group start to weigh three difference empty test tube to get their mass before we put any unknown salt in so we don’t make a calculated mistake. Zeroing the balance with the beaker inside, we put the test tube in the beaker to calculate the unknown hydrate mass.
Then, 5 mL of the halved concentrated solution was measured and added into another volumetric flask. 5 mL of deionized water was added to produce a solution that was a fourth of
There is one mole of OH- in the solution since NaOH goes to Na+ and OH-. Trial 1: 25.65mL NaOH x 0.100mol/1000mL = 2.57 x 10-3 mol NaOH = 2.57 x 10-3 mol HA = 2.57 x 10-3 mol H+. The equivalent mass is 0.356g Acid / 2.57 x 10-3 mol H+ = 139g/mol H+ Trial 2: 49.57mL NaOH x 0.100 mol / 1000 mL = 4.96 x 10-3 mol NaOH = 4.96 x 10-3 mol HA = 4.96 x 10-3 mol H+. The equivalent mass is 0.644g Acid / 4.96 x 10-3 mol H+ = 130.g/mol H+ Average =
Label the test tubes with hot Using a test tube holder put the test tubes into the beakers. Place 2 test tubes with the hot label in the hot water and the other 2 with the cold label in the ice. Let the test tubes be in the beaker for 5 minutes. Take all the test tubes out of the beaker and drain the water. Then add 3 ml of hydrogen peroxide using a pipette to all the 4 test tubes.
= 10^-3 M = 1,000 mL Here C1,C2; are the first and second concentrations of solution V1 and V2 ; are the required and current volumes. The impeller turned on and DDA, and tap water left to be mixed properly with water for 2 minutes. Approximately 150 grams of quartz added into the solution.
Weighed 1 gram of NaC2H3O2 and mixed it with ionized water. Boiled 12 mL of 1.0M Acetic Acid added into a beaker containing the sodium carbonate on a hot plate until all the liquid is evaporated
Move 10 ml of the fourth well to the fifth well. FIll the fifth well with 90 ml of dh20 to reach 100ml. Start with 1% solution for Fluoride 100 ml and move 10ml of the first well into the next. Fill the well with 90ml dh20 to reach 100ml. move 10 ml of the second well to the third well.
The volumetric flask was then filled up to its 100 mL mark with deionized water. The buret was washed out with dionized water and then with the strong base NaOH before being filled up with NaOH. About 20 mL of the unknown weak acid was pipetted into a beaker. The starting volume of the NaOH in the buret was recorded before about 4 mL of the strong base was titrated into the weak acid solution. The final volume was recorded.
5. Join the side arm flask to source of vacuum. While dealing with this experiment you should always use thick walled tubing, the pressure will collapse with the Tygon tubing. 6. Wet the filter paper with a tiny amount of solvent to be used in the filtration.
Again select the flask and select Distillation Head from the drop down menu. ➢ For the third time select the flask and choose Condenser from Distillation from the menu and for last time select the flask Distillation Take-off from the dropdown option. ➢ Select the 100 mL Graduated Cylinder from the Equipment option and put it underneath of distillation take-off.
Weight a clean, dry, porcelain evaporating dish on the electric balance and record this mass on an appropriate data table. If the crucible needs to be washed before use, then heat the crucible in the Bunsen burner flame for a few minutes and remove any residual water. Then allow it to cool before continuing. Fill the crucible about 1 gram with the hydrated salt and reweight. Assemble the ring stand, ring, clay triangle, and Bunsen burner
(Molarity)(Volume)(Molar mass) The pellets were dissolved thoroughly then was used in filling up the 100 mL volumetric flask. The solution was mixed well
Once dissolved, fill the rest of the volumetric flask up to the line on the neck of the flask. Again mix the solution. Use four, 10mL volumetric flask, and label them from 1-4. Add approximately 2mL of copper sulfate pentahydrate into flask 1, 4mL to flask 2,
The drop rate was adjusted to 1 to 2 drops/second. 10.0 mL of the NaOH solution was allowed to drip away into a waste beaker. The exact volume of the sodium hydroxide solution used was determined.