Effect of preparation conditions on the catalytic activity of CuMnOx catalysts for CO oxidation The oxidation of carbon monoxide to carbon dioxide was an important procedure and it’s used in various fields such as respiratory protection, automobile emissions control, industrial air purification and fuel cells etc. The main aim was on the enhancement of the catalytic activity for low temperature CO oxidation. The CuMnOx catalyst was a well known catalyst for low temperature CO oxidation. The experimental parameters like molar ratios of precursor, particle size, drying temperature, drying time, calcination temperature and calcination time has influence on the activity of catalyst performance. Activity of the catalyst was measured in flowing air …show more content…
A lot of interest has been given to modification of the CuMnOx catalyst to remove its faults of moisture for deactivation and lower activity (9). The Optimization during the preparation conditions like drying temperature, drying time, calcination temperature, calcination time and the molar ratio of (Cu:Mn) in CuMnOx catalyst have been increased the performance of CuMnOx catalysts for CO oxidation at a low temperature (10). In this paper, we have to investigate the effect of a broad range of preparation parameters to enable the optimal catalyst preparation procedure to be …show more content…
The particle size of the catalyst also influenced the activity of the resulting catalyst, with the decreasing of the particle size; the surface area of the catalyst was increased therefore more CO oxidized into CO2 gas (12). The drying temperature, calcination temperature and calcination time has a distinct effect on the catalyst performance and its structure was analysis by TGA and X-ray diffraction results (13). There were many things, which can be varied during the catalyst preparation by co-precipitation method and the subsequent calcination step for controlling the activity of the catalyst for CO oxidation (14). To date, they are various methods have been applied to the preparation of CuMnOx catalysts; it’s including sol-gel, ultrasonic aerosol pyrolysis, co-precipitation, supercritical antisolvent precipitation and the reduction methods. In the above methods the co-precipitation method, can produce the highly active sites of the CuMnOx catalyst
3.1 Project Methodology In order to make sure that this project is on track, proper planning and scheduling is crucial. It is necessary to identify the significant key points which are photocatalytic activity of SWCNTs, properties of carbon nanotubes and titanium oxide, available testing procedures using scanning electron microscopy (SEM) and other spectroscopic methods. In this section, a brief detail provided regarding the methods used, sol-gel, hydrothermal and electrospinning. Also, the available tests that will be used are explained.
The reaction was repeated 3 times and average rate noted. From these rates a graph was plotted which describes the relationship of the pressure produced and number of drops added. The reaction rates were measured by Kpa/min and were written to 4 figures for precise results. Time was measured by stop watch. Table 4 shows a summary of all the groups which participated in the lab session.
K.D.A. Saboia et al. , (2007) have been prepared the Bi4Ti3O12–CaCu3Ti4O12 {[BIT(X)–CCTO(100-X)]} composite powders through solid state reaction method and calcined in the range of 900 to 1020 ºC for 12 h. The as-prepared powders have modified in the form of thick film onto alumina ceramic substrate by utilizing screen printing. At 100 Hz, the value of dielectric constant (κ) of CCTO100 and BIT100 is 316.61 and 53.64 respectively. Conversely, the composite with X=20 % shows an unexpected dielectric constant of 409.71, which is around 20% higher in comparison with the CCTO.
Name: Avishak Deb Roy Partners: Leevell Penn, Varugh, Butler Bio 101 Lab Report #1 02.22.2018 Swimming speed of paramecium tetraurelia in different levels of treatment. Introduction Paramecia is a unicellular Protista which are naturally found in aquatic habitats. It is easily cultured in the laboratory. It is oblong shaped and covered with short hairy structure called cilia. Paramecia does not pose any health or ethical concerns and the population can be maintained if there is a food source such as Enterobacter (Biological Foundation 7).
A transfer pipette was used to place a single Daphnia magna into the well of a concave slide and any excess water was removed by using a Kimwipe tissue. The use of a coverslip was unnecessary so that the specimen isn’t crushed and killed. The D. magna had enough water to allow its gills to function but not so much that it could’ve actively swim. The specimen’s heart was located using a light microscope using the lowest magnification.
Prove if the material in cup 6 is a metal, metalloid, or nonmetal, by using its appearance, color, state of matter, luster, conductivity, malleability, and how it reacts with HCL. Before beginning to test on the substance we observed its appearance, state of matter, luster, and color. The substance was very shiny, solid and hard, as well as silver. Then we put on safety goggles to start testing.
Genetic engineering is changing the DNA code to express different traits. A plasmid is a circular piece of DNA that contains important genetic information. Recombinant DNA is the product after inserting your desired genes. The genes we hoped to insert in the pGLO lab were the GFP gene and the ampicillin resistance gene. GFP was needed so that we would tell if the ampicillin resistance gene had been properly placed when the bacteria glowed under a UV light.
ST Report In the experiment, the problem was the contaminants that were affecting the quality of the water samples. To fix this issue, three scientists had to determine the contaminants that were present in the samples. One sample was from the school sink and the second sample was from an unknown source. The scientists conducted many tests to figure out what pollutants were present in the water.
Elodea is a type of rooted plant with multiple branches (Elodea). Elodea is known as a weed located in parts of Australia, Africa, Asia and Europe, but is known to be popular in Washington’s lakes, ponds and rivers (Native Freshwater Plants, 1994). Photosynthesis involves light energy converting to sugar while respiration burns the sugars produced in photosynthesis in order to help the plant grow and reproduce (Whiting, 2014). The equation for photosynthesis is 6CO2+ 6H2O⇢C6H12O6+ 6O2. In other words, carbon dioxide, water and light are the reactants, and the products of photosynthesis are glucose and oxygen.
With many factors affecting chemical reactions, there is a significant relationship between these factors and the rate that they occur. As seen through many studies and experiments, surface area of solid reactants has a great impact on this rate of reaction. In conclusion, the scientist has learned important relationships and factors involved in the rate of which chemical reactions
The purpose of this lab was to test the effect of pollution on algae growth. Through a series of experiments that lasted a month, four of the six hypotheses were proven to be correct or partially correct. The first hypothesis stated that if 0.5 mL of salt was added to algae, then the algae would grow slower than the positive control. This was proven correct, as shown by the difference of the data from the positive control and the container with 0.5 mL of salt in it.
Quinn Nguyen Floating Leaf Disk Photosynthesis Lab Conclusion: Graph your results for all 3 trials on one graph. Label the graph, both axes, and provide a legend to distinguish each trial. What was the rate of photosynthesis for each variable? How many leaves floated per minute? Rate of photosynthesis (leaves/min) Spinach: (2-0)/25 = 0.08
1. This experiment was performed using cells from 3 different species, Vicia faba (broad bean), Allium cepa (onion), and Coregonus clupeiformis (whitefish), which obviously have variability between them. Onions are bulb plants, meaning they have a ball of stored nutrients underneath the soil out of which the roots protrude, where the broad bean does not have a bulb, having most of its mass above the soil. The whitefish is of course an animal, entirely different from the plants, including in how the cell cycle is performed. A cleavage furrow forms instead of a cell plate to perform cytokinesis, and centrosomes are present in its mitotic cycle, unlike in plants.
Doriana Spurrell What different frequencies and types of light would prompt the Spinach leaves to go through the process of photosynthesis effectively? Purpose: The purpose of this experiment was to see which of the four lights that range across the light spectrum would properly and most efficiently help the spinach leaf perform photosynthesis. Background Information: Photosynthesis is the process in which plants use light energy to transform into chemical energy.
The decomposition of NaHCO3 is an example of Prevention within Green Chemistry principles because all solid waste in this experiment is collected and used again. The only gaseous wastes generated by the reaction in the experiment are carbon dioxide and water, which are benign (Lab 3). The decomposition reaction of NaHCO3, generates virtually no waste, therefore less hazardous chemical syntheses. The byproducts of the reaction are gaseous CO2 and H2O which possess little or no toxicity to human health and the environment, because of the amounts released in this experiment. (Lab 3).