4.1 Distillation Column Design (Hazel Villarosa Victorio -1415939) 4.1.1. Introduction and design statement Chemical engineers have a part to play in achieving sustainable goals. Since natural resources are scarce and depleting, improvement of chemical processes is important. Recovering and reusing raw materials to convert into finished products is one of such simple techniques. In production of Acetone through Isopropanol, this goal of recovering and reusing of materials can be achieved. Isopropanol (IPA) is a key chemical used for production of Acetone through dehydrogenation. However, only a fraction of Isopropanol is converted to Acetone. Therefore, it is necessary to recover as much IPA from Acetone Bottom Product through distillation process. Distillation is a mass transfer unit operation that separates components of a liquid mixture based on the differences in volatility or boiling point of the components. It involves …show more content…
Theories and methodology in distillation column design Theory Tray column is a cylindrical vessel containing a series of trays. Mass transfer between liquid and vapour occurs on trays in cross-current under a certain pressure. There are different types of trays such as valve trays, bubble cap trays and sieve trays. Valve trays are trays that has holes which are covered by caps that are lifted up by the vapour flowing into the holes. This provides excellent contact between liquid and vapour. A decrease in vapour flowrate will cause the cap height to decrease as shown below: Bubble cap trays are trays that has a riser and a mounted cap for each hole (Figure 4.1.2). This forces the vapour to flow downwards and rise again, forming bubbles once it contacts with the
The dehydration of 2-methylcyclohexanol takes place at the bottom of the Hickman still. As the Hickman still heats up within the sand bath, the products evaporate and travel higher up in the still where they condense into a liquid and fall within the collection ring, thus separating the product from the remaining water. Drierite (CaSO4) is also added as a drying agent to absorb any leftover water within the product. The purity of the product will then be analyzed with infrared spectroscopy, paying attention to OH peak if it is present. Chemical Reactions: Data and Observations: Material Volume Mol.
Lab Report 5: Acetylsalicylic Acid (Aspirin) Synthesis Name: Divya Mehta Student #: 139006548 Date Conducted: November 19th 2014 Date Submitted: November 26th 2014 Partner’s Name: Kirsten Matthews Lab Section: Wednesday 2:30 L9 IAs Name: Brittany Doerr Procedure: For the procedure, see lab manual (CH110 Lab Manual, Fall 2014) pages 96-98. Wilfrid Laurier University Chemistry Department. Fall 2014. Acetylsalicylic Acid (Aspirin) Synthesis.
Pop Rocks and soda have a very interesting chemical reaction with each other. Soda is a very pressurized drink that has carbon dioxide in it. Carbon dioxide is a pressurized chemical. When it is shaken, it fizzes, and causes pressure, and overflows releasing the carbon dioxide. It is similar to the Pop Rocks.
In this lab we used two processes called Diffusion and Osmosis. Diffusion is the movement of molecules from areas of high concentration to areas of low concentration. Diffusion is a process that requires no energy and involves smaller non-polar molecules. In Figure 1 you can see the molecules spreading throughout the glass from the area of high concentration, so that the areas with low concentration are filled evenly as well. The other process was osmosis.
The fractions in the fractional distillation such as N-hexane, isohexane, methyl cyclopentane have normal boiling point close to cyclohexane which makes the recovery of cyclohexane uneconomic and difficult. 2. Quantity of cyclohexane recovered is not enough to meet the current demand since the cyclohexane content of naphtha is about 5%- 15% by weight .3 Selection of Pathway to Cyclohexane (2) Hydrogenation of Benzene: C6H6 +3H2 →
Again select the flask and select Distillation Head from the drop down menu. ➢ For the third time select the flask and choose Condenser from Distillation from the menu and for last time select the flask Distillation Take-off from the dropdown option. ➢ Select the 100 mL Graduated Cylinder from the Equipment option and put it underneath of distillation take-off.
The malt holder will hold it there and pass warm air through it again, to make sure that it’s nice and dry before it is passed to the next area of the
The thermal distillation process uses heat to evaporate water and then later liquefy again. When there is leftover heat or enough electricity available, as is often the case with factories and power plants, thermal distillation is a well-organized and workable
Purpose/Introduction The process of recrystallization is an important method of purifying a solid organic substance using a hot solution as a solvent. This method will allow the separation of impurities. We will analyze Benzoic Acid as it is dissolved and recrystallized in water and in a solvent of Methanol and water. Reaction/Summary
Commercial vinegar, Yamaha brand 0.1 mol/dm3, NaOH soloution Phenolpthalein indicator soloution (50.00 ± 0.5 cm3 ) cm3 burrete (250.00 ± 0.5 cm3) volumetric flask a (250 cm3± 0.5 cm3)
that could not otherwise fit in the small space between stackable trays. You can also make yogurt in your own jars in a shelf dehydrator that would not be possible in a stackable dehydrator. Though the stackable dehydrators don't have much clearance between trays, they do have an advantage that the shelf dehydrators don't have: expandability. Stackable dehydrator models usually come with 4, 6, 8, or 10 trays right out of the box. However, you can purchase additional trays to increase the capacity of your dehydrator as your dehydrating needs grow.
DETERMINATION OF PERCENTAGE ETHANOL IN BEVERAGES 1. Introduction to Gas Chromatography Gas chromatography is a very powerful separation technique for compounds that are reasonably volatile. The components of a sample partitions into two phases, the 1st of these phases is a immobile bed with a great surface area, and the other is a gas phase that permeates through the immobile bed. The sample is evaporated and passed by the mobile gas phase or the carrier gas through the column. Samples separates into the stationary liquid phase, based on their solubilities at the given temperature.
Introduction Buffer is a solution that resists a change in pH when bases or acid are added. Solutions that are acidic contain high concentrations of hydrogen ions (H+) and have pH values less than seven. Buffer usually consist of a weak acid, and its conjugate base or a weak base and its conjugate acid. The function of buffer is to resist the changes in hydrogen ion concentration as a result of internal and environmental factor. This buffer experiment is important so that we relies the important of buffer in our life.