DESCRIPTION
FIELD OF THE INVENTION
The invention involves the usage of electromagnets for reducing the viscosity of paraffinic crude oil. It also focuses on the behaviour of the various rheological parameters of crude oil such as Relaxation Modulus, Shear Stress, Strain and Deflection Angle after removal from short termed magnetization.
BACKGROUND OF THE INVENTION
Viscosity of the fluid is defined as the a measure of resistance to the gradual deformation by shear stress. Viscosity arises from the friction between the neighboring particles in fluid moving with different velocities. It is a governing factor for transporting the crude through the pipeline over large distances and it differs from 5 cP - 100,000 cP, depending upon the composition
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Hence, paraffins tend to solidify when they come from reservoir (rock) to the surface conditions. This phenomena results in the deposition of paraffins inside the tubing which results in choking and causes hindarance in the fluidity of crude through the pipelines. Apart from crude composition and temperature, pressure and particle agglomeration also affects the viscosity factor of paraffinic crude.
Some of the conventionally methods have been mentioned which are used to reduce the apparent viscosity of crude oil.
1. Thermal methods include either heating of pipelines or injecting some hot fluids (water / polymer) with crude.
2. Chemicals are also used to reduce the viscosity of waxy crude by altering the thermodynamic properties and pour point or by modifying the larger paraffinic crystals into the smaller ones.
3. Viscosity of waxy crude is also lowered by applying the sudden jerks below their pour point.
SUMMARY OF THE
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The Viscometer was replaced with the Rheometer so that other rheological properties of crude can also be studied after magnetic treating.
2. Florescence Microscope (see figure 6) was used to study the effect of magnetic field on the crude at the microscopic level (see Figure 7 & 8).
The procedure of the experiment was described below:
1. The crude sample was heated at the 46° C in the hot air oven (see Figure 9) and the temperature of water bath was kept at 50° C in order to maintain the constant temperature during magnetic treating.
2. The crude was treated for 1 minute at different magnetic fields (6500, 7500 and 8500 Gauss) for 3 times (see figure 10) to ensure the repeatability of the field.
3. Finally, the sample was placed in Rheometer which was maintained under constant temperature (46° C) and shear rate (34 s-1)for 150 minutes (2 hours 30 minutes).
The Aton Parr Rheometer was selected for conducting the experiment. The Sensor Probe (SN33439) was 38.719 mm in diameter and 60.012 mm in length. The radius of the cup used for storing the crude oil sample was 21.000 mm with the measuring gap of 1.641 mm. The cone of the probe was making an angle of 120°.The volume of the crude sample filled in the Rheometer cup was 58 ml. The probe was recommended for viscous fluids (μ > 50
The magnetized zeolite was then cooled for 5 minutes. For both zeolite and magnetized zeolites, the solutions were placed in two centrifuges with equal amounts of solution and placed in both tubes. The tubes were placed in the centrifuge for 10 minutes at 5000 rpm. The liquid in the tube after the centrifuge was poured into a 200 mL waste
The purpose of this lab was to be able to use physical characteristics to determine the identity of an unknown compound. The data from this experiment classified aluminum as metallic; ascorbic acid, paraffin, palmitic acid, sucrose, graphite, and water as molecular; sodium chloride as ionic. In order to determine this, 3 tests were conducted. The first test was to test the conductivity of each substance at room temperature. In this test, only graphite and aluminum conducted.
Characteristic Property- Test 2- Density Materials: Triple Beam balance, distilled water, graduated cylinder, unknown 6 Procedure: first we found the mass of the empty graduated cylinder and then its mass with the now distilled unknown. After subtracting the mass of the graduated cylinder, we were able to find the volume. For every 1mL=1cm³ so there we had the volume found with the graduated cylinder. We divided the mass by the volume in order to get the density Data: We found that the density of our unknown was 0.76 g/cm3.
Pipelines are also proven to be the safest method of transferring crude oil,
less damage in the pipeline can cause the environment to be clean and to allow the people not to be worried and to think that the pipe can transport the crude oil
The goal of experiment four was to use sodium dichromate to oxidize borneol to camphor. To purify the camphor use sublimation, then reduce camphor to isomeric alcohol isoborneol with sodium borohydride. Use the 1H NMR to determine the ratio of borneol to isoborneol in the final product. The experiment was carried out by using sodium dichromate to oxidize a borneol solution that was made with borneol and ethyl acetate. Once the reaction was complete the mixture was transferred into a separatory funnel where the ether and aqueous layers were separated and the aqueous layer was then extracted with two portions of ether.
The dehydration of 2-methylcyclohexanol takes place at the bottom of the Hickman still. As the Hickman still heats up within the sand bath, the products evaporate and travel higher up in the still where they condense into a liquid and fall within the collection ring, thus separating the product from the remaining water. Drierite (CaSO4) is also added as a drying agent to absorb any leftover water within the product. The purity of the product will then be analyzed with infrared spectroscopy, paying attention to OH peak if it is present. Chemical Reactions: Data and Observations: Material Volume Mol.
Modifications of this procedure include the use of hot plates instead of Bunsen burners, and heating t-butyl alcohol to 60-65 ℃ instead of 50 ℃. Other modifications include the use of weighing boats to measure an amount of unknown instead of weighing paper, and completing one run of unknown 2 instead of two runs of unknown 2. Summary of
Synopsis This laboratory report gives an outline of the experiment which was carried out in order to measure the density of water at different temperatures via two different methods. The lab consisted of two parts. In the first part the density of water was measured by hydrometer. At first the density of water at room temperature was measured.
The crude oil is heated in a tall cylinder called fractionator for at least 350 degC. The process is based on the principle that different substances boil at different temperature. The cyclohexane content of naphtha fraction of crude oil can vary from 0.5 to 5.0 volume %. N-hexane, isohexanes, methyl cyclopentane, benzene and dimethyl pentanes have normal boiling points very close to cyclohexane.1 Advantages: 1. Uses a simple method of cyclohexane recovery. Disadvantages: 1.
Rediet Legese iLab Week # 6 CRUDE OIL DISTILLATION Introduction: The aim of this week lab experiment is to experiment distill crude oil and to check how temperature determine the chemical properties of crude oil plus how the boiling point can also show physical properties. They are two major finding in this experiment. he first finding was the point at which the raw petroleum is heated to the point of boiling, at 275 0C, the gas and kerosene oil are refined, however the oil (lubricant ) stays as an unrefined feature oil.
The developing solution was poured into a tank and was tightly covered with a glass lid, and the tank was allowed to be saturated to ensure that the solution was equilibrated in the gas phase. Silica plate for TLC analysis: A horizontal line was drawn with a pencil on the plate and it was about 1 cm above the bottom of the plate. The horizontal line was drawn faintly so as to avoid damaging the silica gel on the plate. On the horizontal line, two marks were made and one was named A and the other B. These marks were made towards the centre of the plate at a distance apart because when spots are made at the edge of a plate, the result would be an improper travel of the samples as the solvent advances on the plate.
II. METHODOLOGY In order to perform this experiment, the students will need a distillation set-up with a connector receiver, an iron ring and stand, a Bunsen burner, a wire gauze, a 250mL round bottom flask, a graduated cylinder, a thermometer, one or two boiling chips, an alcoholic beverage, masking tape, an ice bath, a stirring rod, and, optionally, food coloring. It is imporatnt to avoid playing with the apparatus and equipment so as to avoid breakage and injuries, especially since fire is being dealt with in this experiment.