CHAPTER 3
EXPERIMENTAL INVESTIGATION
3.1 General
The experimental work was done to evaluate the effect of waste glass powder on the technical properties of concrete. The waste glass generated from glass industries and basically generated from broken doors and windows are grounded fine and used for the partial replacement of cement. For studying the effect of glass powder on compressive strength of concrete, density and water absorption, 150mmX 150mm X150 mm specimens were casted by partially replacing the cement from 0% to 25 % with an interval of 5%. Similarly the beams of size 100mm x 100mm x 500 mm were casted to determine the flexural strength of the cement. The mix design was prepared as per IS 10262:2009. The specimens were casted and
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Adjust that it shows zero reading when touches the non-porous plate. The plunger is released and reading is noted.
Quantity of cement = 400gm
Quantity of water in %, P = 33% Figure 3.1 VICAT APPARATUS
3.3.1.2. Setting time Test
Vicatapparatus with 1mm2needle is required for this experiment.
The time consumedfrom the addition of water in cement to the point at which needle fails to penetrate the test sample to a depth of 5mm from the bottom is known as Initial Setting time. While Final Setting time is the time consumed from the addition of water in cement to the time at which needle of 1mm2 with 5 mm diameter attachments fails to make an impression on the sample.
PROCEDURE:
A sample of 400gm is taken. 0.85 P % water by weight of cement is added and mixed, where P is normal consistency. Fill the Vicatmould and level the surface of the mould. The gauging time should be in between 3 to 5 minutes. The needle is brought near the top surface of cement paste and released. Step d is repeated till the needle fails to penetrate the cement paste about 5mm from the bottom of the mould.This time, is noted and is Initial setting time. The needle is replaced by the angular
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The test is performed to determine the fineness of cement i.e. whether the cement is properly grounded or not. Finer the particle, higher will be the rate of hydration and the development of strength will be quick.
PROCEDURE:
Take 1000 gm of cement and place it on 75µm sieve. The cement is sieved and the weight of cement-retained on the sieve is noted. Calculate the percentage retained and should range from 0 – 10%.
Table 3.2 FINENESS OF CEMENT
Observations Test 1 Test 2 Test 3
Weight of cement, gm 1000 1000 1000
Weight of cement-retained, gm 40 35 37.5
Percentage Weight retained, % 4% 3.5% 3.75%
Average % Weight retained 3.75%
3.3.1.4 Specific Gravity
The specific gravity of cement is defined as the ratio of the weight of a given volume of cement to the weight of an equal volume of water.
The specific gravity bottle is used for this experiment.
PROCEDURE:
The weight of empty bottle is noted i.e. w1. Now the bottle is filled with distilled water and the weight is noted i.e.
Prelab week 1 Calculations Preparation of 1.5μmol/L mixed low-level standard dilution 150μmol/L × V1=1.5μmol/L × 10ml V1=(1.5μmol/L×10ml)/(150μmol/L)=0.1ml Conversion of milliliters to microliters (0.1ml×1000)μL= 100μL Preparation of 3μmol/L mixed low-level standard dilution 150μmol/L × V1=3μmol/L × 10ml V1=(3μmol/L×10ml)/(150μmol/L)=0.2ml Conversion of milliliters to microliters (0.2ml×1000)μL= 200μL Preparation of 3μmol/L mixed low-level standard dilution 150μmol/L × V1=7.5μmol/L × 10ml V1=(7.5μmol/L×10ml)/(150μmol/L)=0.5ml Conversion of milliliters to microliters (0.5ml×1000)μL= 500μL Preparation of the blank samples The volumetric flask will be filled to the mark with 150μmole/L of stock solution to act as blank (reference). Additional two blanks will
Characteristic Property- Test 2- Density Materials: Triple Beam balance, distilled water, graduated cylinder, unknown 6 Procedure: first we found the mass of the empty graduated cylinder and then its mass with the now distilled unknown. After subtracting the mass of the graduated cylinder, we were able to find the volume. For every 1mL=1cm³ so there we had the volume found with the graduated cylinder. We divided the mass by the volume in order to get the density Data: We found that the density of our unknown was 0.76 g/cm3.
The resin that had stuck to the sides of the burette was washed down by pipetting extra pH 3 citrate buffer along the sides. The column was tapped to ensure that the settled resin formed a level surface. After all of the resin settled, the buffer was drained into a waster beaker until the level of the buffer reached the top surface of the resin. For the remainder of the experiment, the top surface of the resin was not allowed to dry
Further experimentation could be done, to reduce the risk of errors within the measuring of the absorbance of standards which may have occurs. If the error of not wiping the cuvette
In the experiment they used probes to test for pH, dissolved oxygen, total dissolved solids, conductivity, and turbidity. The probes hook up to the computer and collected the averages for each test. They collected this data and used it for later evaluation of the contaminates. They also tested for iron, copper, and chlorine with different tablets.
= 10^-3 M = 1,000 mL Here C1,C2; are the first and second concentrations of solution V1 and V2 ; are the required and current volumes. The impeller turned on and DDA, and tap water left to be mixed properly with water for 2 minutes. Approximately 150 grams of quartz added into the solution.
These small errors may be arised as a result of temperature. Because the accurate mesuring process took much time and during this time the temperature of water was decreasing. Among two methods the density bottle gives more accurate measurement of the volume, resulting in more accurate determination of density. One of disadvantages of hydrometer is that hydrometer has Operator dependent readings, therefore has limited accuracy. Morever, for measuring the density using hydrometer large sample volume is required.
Materials and Methods The chemicals used to perform this experiment were distilled water, sodium chloride (NaCl), ice,
Second, the experimenters has to fill up a measuring cup until the water reaches 200 mL. Third, the experimenters will fold the paper towel in half three
interface which plugged into a computer and Logger Pro opened. To calibrate the probe, Experiment-Set Up Sensors-Showed All Interfaces was selected and then Calibrate Now was on. The probe was cleaned in distilled water and dried. Then the probe was placed into a buffer solution. There was two buffer solutions, one with a pH of 4.00 and the other with a pH of 7.00.
Rinse the sensor in the tap water and then in all three distilled water bowls. Repeat steps 1–13 in the "Measuring the Conductance" section two more times to obtain a total of three measurements for each liquid. Average the current measurements of the three trials of the
Literary Analysis: “The Rose That Grew From Concrete” by Tupac Shakir Everyone in the world has a form of setbacks and problems, typically with the desire to overcome that. Tupac Shakir’s poem “The Rose That Grew From Concrete” is about a rose that symbolizes a person who defies all expectations. The “flower” succeeds and flourishes despite its disadvantage of growing out of the concrete. True determination leads to success, as conveyed in this poem.
15) After each cuvette was tested, place the distilled water sample (Cuvette zero) to reset the spectrometer and to ensure that the scale is calibrated and repeat for each cuvette test. Data/Results: Tube Number Concentration Of CoCL2 (Mg/ML) CoCL2 Stock (ML) Distilled Water (ML) Spectrometry Reading at
We set those materials in a neat, orderly fashion on our table. Next, we put on our safety goggles. Next, we placed one Magnesium metal ribbon into the 125 milliliter Erlenmeyer flask and we poured 20 milliliters of hydrochloric into the graduated cylinder. Then we placed the 125 milliliter Erlenmeyer flask with the magnesium, the rubber stopper, and the graduated cylinder with 20 milliliters of hydrochloric acid onto a scale. After we got the different masses, we added them up until we got a final total and we put that mass into a table.
The comb was then placed into the solution to create the wells. Once the gel had solidified (4-5 minutes) the comb was carefully removed. The solidified gel was then placed into the buffer chamber ensuring that the wells were located closest to the negative terminal. This ensures that the DNA will travel through the gel in the direction of the positive terminal. If the wells are placed closest to the positive terminal it will result in the DNA running off the gel and a failed procedure.