Misbah Rashid
Candidate Number: 004438-0065
Mrs. Angela Arnold
Chemistry HL
16th November 2014
IB Chemistry Internal Assessment
Determining the Concentration of Ethanoic Acid in Vinegar
DCP and CE
Data Collection and Processing
Raw Data Rough titre First accurate titre Second accurate titre Third accurate titre
Initial burette reading Vi / cm3 (±0.05 cm3) 7.60 6.20 5.60 3.40
Final burette reading Vf/ cm3 (±0.05 cm3) 34.1 32.2 31.9 29.1
Total titre Vacid / cm3 (±0.10 cm3) 26.5 26.0 26.3 25.7
Concentration of NaOH 0.1 mol dm-3
Volume of Vinegar /cm3 (±0.12 cm3) 25 cm3
Phenolphthalein indicator 3 drops
Qualitative data: The pink color of phenolphthalein indicator and sodium hydroxide solution turns colorless when it reaches the end point.
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Diluted vinegar is titrated against sodium hydroxide solution and the volume of diluted vinegar is obtained through calculation.
Error Analysis
The literature value provided was 5%. The result that was attained from the experiment was (6.006 ± 0.05)%.
Percentage error = ((5-6.006)/5)×100 = 20.12%
The percentage error has a wide difference from the percentage uncertainty acquired from the apparatus, which was 0.908%. Therefore, the result of the experiment does not agree with the literature value and is not suitable.
Evaluation
Weakness/Limitation Why? Suggestion
Sodium hydroxide left in the pipette Few drops of NaOH might have been left in the pipette while transferring it to the conical flask. If some of it remains, there is a systematic error and the expected amount of moles in conical flask is lesser. Hence, the amount of ethanoic acid to neutralize sodium hydroxide is lesser too. Distilled water can be poured in the pipette to swill out the remaining sodium hydroxide. Distilled water will not affect the amount of moles in sodium hydroxide, but it will remove the remaining NaOH in the pipette and transfer all in the conical
A hot plate was placed under the ring stand. 50 mL of 3.0 M NaOH in a 250 mL beaker and a stir bar was placed in the beaker. The beaker with NaOH was placed on the hot plate and 3.75 grams of NaAlO2*5H2O was placed in the beaker. The temperature probe was placed in the beaker with the solution, not touching the bottom of the beaker. The solution was heated and stirred till the solution dissolved.
After obtaining an homogeneous mixture, the flask was placed in an ice bath during five minutes next to a graduated cylinder containing 5.0 mL of concentrated sulfuric acid. The temperature of the ice bath was recorded to be 1.1 °C. Likewise, a second graduated cylinder containing 1.8 mL of nitric acid and 2.5 mL of sulfuric acid was immersed in the cold ice bath to keep the three different solutions at the same temperature. Thereafter, the cold 5.0 mL of H2SO4 were added to the erlenmeyer flask containing the acetanilide solution, which remained in the cold water for approximately another 4 minutes.
Wt. Mass Density Appearance 2-methycyclohexanol 0.75 mL 114.19 g/mol 0.93 g/mL Clear colorless liquid 85% Phosphoric acid 1.00 mL Clear
Weighed 1 gram of NaC2H3O2 and mixed it with ionized water. Boiled 12 mL of 1.0M Acetic Acid added into a beaker containing the sodium carbonate on a hot plate until all the liquid is evaporated
The soda water will be stored in 5 different temperatures : 5℃, 15℃, 25℃, 35℃, and 45. The desired temperatures will be achieved by using the water bath and refrigerator. I chose phenolphthalein as the indicator, because it is commonly used for titration and is a weak acid. Phenolphthalein is usually used when the solution is strong base and weak acid. When it is added into an acidic solution, the solution will be colourless; when it is added into an alkaline solution, the solution will turn pink.
Stoichiometry is a method used in chemistry that involves using relationships between reactants and products in a chemical reaction, to determine a desired quantitative data. The purpose of the lab was to devise a method to determine the percent composition of NaHCO3 in an unknown mixture of compounds NaHCO3 and Na2CO. Heating the mixture of these two compounds will cause a decomposition reaction. Solid NaHCO3 chemically decomposes into gaseous carbon dioxide and water, via the following reaction: 2NaHCO3(s) Na2CO3(s) + H2O(g) + CO2(g). The decomposition reaction was performed in a crucible and heated with a Bunsen burner.
Empirical Formula of Magnesium Oxide - Lab Report Background Information/Introduction: The aim of this lab is to determine the empirical formula of magnesium oxide by converting magnesium to magnesium oxide. As an alkali earth metal, magnesium reacts violently when heated with oxygen to produce magnesium oxide and magnesium nitride as a byproduct. In order to obtain only magnesium oxide, distilled water was added so that magnesium nitride will react and convert to magnesium hydroxide. Further heating then oxidizes all of the magnesium into magnesium oxide.
CONCLUSION When you put an egg in vinegar, we see that the shell dissolves, but do you ever wonder why? An egg is made mostly out of calcium carbonate which reacts with an ingredient in vinegar, acetic acid. Acetic acid is about 4% of the vinegar and what breaks apart the solid calcium carbonate crystals. The bubbles we see, from the egg, is the carbonate that make carbon dioxide and the other calcium ions float free. This is the equation: CaCO3 (s) + 2 HC2H3O2 (aq)
How does the amount of baking soda mixed with vinegar affect the volume of gas produced? The rate of reaction is the increase or decrease time taken at which the products are formed or concentration increase or decrease between a reaction of two or more substances. In the reaction, new bonds are formed whilst others have been broken.
Commercial vinegar, Yamaha brand 0.1 mol/dm3, NaOH soloution Phenolpthalein indicator soloution (50.00 ± 0.5 cm3 ) cm3 burrete (250.00 ± 0.5 cm3) volumetric flask a (250 cm3± 0.5 cm3)
Upon cooling, it was shaken until no bubbles were formed. 20 mL of each brand of soft drinks was titrated with NaOH solution. 3 drops of phenolphthalein was used as an indicator if it has already completely reacted. The acidity can then be calculated referring on the known concentration and volume of base; and the known volume of acid.
DETERMINATION OF PERCENTAGE ETHANOL IN BEVERAGES 1. Introduction to Gas Chromatography Gas chromatography is a very powerful separation technique for compounds that are reasonably volatile. The components of a sample partitions into two phases, the 1st of these phases is a immobile bed with a great surface area, and the other is a gas phase that permeates through the immobile bed. The sample is evaporated and passed by the mobile gas phase or the carrier gas through the column. Samples separates into the stationary liquid phase, based on their solubilities at the given temperature.
Synopsis This experiment is the determination of Calcium Carbonate (CaCO3) content in toothpaste with the use of back titration while demonstrating quantitative transfer of solids and liquids. A accurately weighed quantity of toothpaste was dissolved in excess volumes of HCl. This solution is then titrated with NaOH to find the volume of the excess HCl. The volume of HCl reacted, which is found by substracting the volume of given HCl with the volume of excess HCl reacted, can be further manipulated with mole fractions to find the mass of CaCO3 and thus the CaCO3 content in toothpastes.
Introduction The goal of the experiment is to examine how the rate of reaction between Hydrochloric acid and Sodium thiosulphate is affected by altering the concentrations. The concentration of Sodium thiosulfate will be altered by adding deionised water and decreasing the amount of Sodium thiosulphate. Once the Sodium thiosulphate has been tested several times. The effect of concentration on the rate of reaction can be examined in this experiment.
That caused a new initial reading of NaOH on the burette (see Table1 & 2). The drops were caused because the burette was not tightened enough at the bottom to avoid it from being hard to release the basic solution for titrating the acid. The volume of the acid used for each titration was 25ml. The volume of the solution was then calculated by subtracting the initial volume from the final volume. We then calculated the average volume at each temperature.