CHAPTER 3
EXPERIMENTAL PROGRAMME
3.1. GENERAL
The main objet of this experimenta is to compare the properties of concrete made with and without plastic aggregates, that is used as coarse aggregate in concrete mix. Major tests carried out on materials used for casting the concrete samples are discussed in this section, a brief description about mix deign and curing procedure used and at the end, the various tests conducted on the specimens are discussed.
3.2. MATERIALS USED
3.2.1. Cement
Cement is a fine and grey powder. When it is mixed with water and materials such as fine aggregates, coarse aggregates and crushed stone, it make bond with them. Cement and water form a mix that binds the materials together as the concrete harden. Ordinary
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Coarse aggregates
Aggregates which are retained on 4.75-mm IS Sieve conforming IS 383- 1970 are known as coarse aggregate. Coarse aggregate are the main load bearing component of concrete. Locally available coarse aggregate having the size of 20 mm was used in our work. figure 3.4 shows the sieve shaker apparatus used for the sieve analysis of aggregates. Table 3.5 shows the properties of coarse aggregate used in experimental work. For finding the fineness modulus sieve analysis for coarse is being done. In table 3.6 the sieve analysis is described as per the study was done.
Table 3.5 Properties of Coarse aggregates
Sr.no. Characteristics Values
1. Type crushed
2. Maximum size 20
3. Specific gravity 2.75
4. Total water absorption 0.5%
5. Fineness modulus 6.61
Table 3.6 sieve analysis of Coarse aggregates
S.No. IS-Sieve (mm) Wt. Retained (gm) %age Retained %age passing Cumulative % retained
1 80 0.00 0.00 100.00 0.00
2 40 0.00 0.00 100.00 0.00
3 20 447 22.35 77.65 22.35
4 10 415 20.75 56.90 43.1
5 4.75 1055 52.75 4.15 95.85
6 2.36 80 4.0 0.15 99.85
7 1.18 0 0 0 100
8 600 0 0 0 100
9 300 0 0 0 100
10 150 0 0 0
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iii) Mix the dry constituents thoroughly to get a uniform colour and then add water. Place the mixed concrete in the cleaned slump cone mould in 4 layers, each approximately ¼ of the height of the mould. iv) Each layer is tamped 25 times by the rounded end of the tamping rod (strokes are distributed evenly over the cross section). vi) After the top layer is rodded, the concrete is struck off the level with a trowel. vii) The mould is removed from the concrete immediately by raising it slowly in the vertical direction. viii) The difference in level between the height of the mould and that of the highest point of the subsided concrete is measured. This difference in height in mm is the slump of the concrete.
3.5.2 COMPRESSIVE STRENGTH TEST
After 28 days of curing compressive strength test is done. Then cubes are taken to the lab after finishing the curing and density measurement. The samples are entered into the Compressing Testing Machine (CTM) to determine compressive strength after measuring its dimension to determine its contact surface
Coursework Equipment List • Boiling tubes (8) I will use these because this is where I will mix both the sodium carbonate and the strontium nitrate in order to form the precipitate. I need 8 because I am going to add 8 different amounts of strontium nitrate (1-8cm³) to the 8cm³of sodium carbonate. • Measuring cylinder (1) I will use this to measure the 8cm³ of sodium carbonate and the varying amounts of strontium nitrate to put into the test tubes. • Sodium Carbonate (enough to fill 8 boiling tubes with 8cm³/64cm³)
During the interval two patients were censored (2+ and 3+) so that at the end of the interval four patients were still at risk. Since the interval ends with the death of one of those, the chance of surviving the interval is estimated as 3/4. Also notice that at the start of the next interval (4 through 10 years), only three patients were at risk due to the death at the end of the interval. The actual curve plotted from this computation is shown in Fig. 2.3.
Buggin’ Out (Buggy Lab) Purpose - To determine the motion of a battery powered buggy & use the data to determine when the two buggies would collide. Data - Position (m) Displacement (m) Time 1 (s) Time 2 (s) Time 3 (s) Time 4 (s) Average Time (s) Velocity (m/s) 1 0 0 0 0 0 0 -- .5 -0.5 1.74 1.38 1.44 1.66 1.53 -.333 0 -1 3.03 3.00 2.95 2.85 2.96 -.338 -.5 -1.5 4.44 4.28 4.44 4.41 4.39 -.342 -1 -2 5.81 5.25 5.65 5.83 5.64 -.354 3.
2 ½ tab divided in 2 pc 19.5 49.5 ½ tab divided in3 pc 21.4 37.11 ½ tab 19.5 53.22 3 ½ tab divided in 2 pc 19.6 48.41 ½ tab divided in 3 pc 20.6 37.30 AVG ½ tab 18.9 53.51 ½ tab divided in 2pc 19.5 49.09 ½ tab divided in 3pc 20.9
The tower is installed on a precast concrete base designed to match the benches in Harriet’s
Log of Proportional Surviving Vs. Age. 4 different decades are graphed on a logarithmic scale to demonstrate survivorship. From Figure 1 and Table 1 it can be seen, 1900-09 had the greatest survivorship out of the 4 decades. Furthermore, 1930-39 had the smallest proportion of survivorship as no individual was recorded to live past there 70’s
6.8 10 Air Conditioner 0 2.4 0.2 0 0 2.6 Electrical System 2.8 2.4 0.2 0 3.4
Use your results in Data Table 2 to support your answer.
1 1 0 1 0 0 1 Total 1 2 2 1 3 0 3 0 0 3 Average 0.333 0.667 0.667 0.333 1 0 1 0
7) Test tube four contains 7 mL of distilled water and 3 mL of CoCl2. The fifth had 7 mL of distilled water and 3 mL of CoCl2. 8) Test tube five contains 6 mL of distilled water and 4 mL of CoCl2. 9) Test tube six contains 5 mL of distilled water and 5 mL of CoCl2. 10) After all of the test tubes are prepared, they will be put into cuvettes.
Purpose/Introduction The process of recrystallization is an important method of purifying a solid organic substance using a hot solution as a solvent. This method will allow the separation of impurities. We will analyze Benzoic Acid as it is dissolved and recrystallized in water and in a solvent of Methanol and water. Reaction/Summary
(Molarity)(Volume)(Molar mass) The pellets were dissolved thoroughly then was used in filling up the 100 mL volumetric flask. The solution was mixed well
A small amount of sand was added after the layer of cotton. After that, a layer of silica filled almost 1/3 of the column. Finally, another small amount of sand was added just above the silica. The column was given a little tap with an aspirator to make the silica more compact. Figure 2.
Introduction The term chromatography actually means colour writing, and signifies a technique by which the substance to be examined is placed in a vertical glass tube containing an adsorbent, the different segments of the substance traveling through the adsorbent at distinctive rates of velocity, according to their degree of attraction to it, and producing bands of colour at different levels of the adsorption column. The substances least absorbed emerge earliest; those more strongly absorbed emerge later. (Wixom et al., 2011) In chromatography of all types, there is a mobile phase and a stationary phase.