. Experimental 2.1 Catalyst preparation In this paper we have to use different types of nitrate precursors to preparation of the catalysts. The precursors we used to preparation of the catalysts are cobalt nitrate, cerium nitrate, copper nitrate and manganese nitrate. All the chemicals are used for manufacturing of the catalyst are A.R. grade and they are purchased from Otto Chemie Company. The different types of nitrate precursors was used to preparation of the catalyst and they are dried at 120°C for 12 hr in an oven and then calcination at 300oC for 2hr in a furnace. The calcination of the precursors is done just before the activity measurement of the catalyst. The calcination of different nitrate precursors was carried out in three ways; …show more content…
The isotherm was recorded by Micromeritics ASAP 2020 analyzer and the physical adsorption of N2 at the temperature of liquid nitrogen (-196oC) with a standard pressure range of 0.05-0.30 P/Po. 2.3 Catalytic Activity Measurement After annealing the catalyst bed, it was cooled to room temperature in the same conditions as we used for reactive calcination. The CO oxidation was analysis by gas chromatogram to measure the activity of the catalyst. The oxidation of CO was carried out to measure the activity of resulting catalyst. 2CO + O2→2CO2 -------------------- (1) The oxidation of CO was carried out under the following reaction conditions: 100mg of catalyst with feed gas consisting of a lean mixture of 2.5 vol.% CO in air and total flow rate is maintained 60 mL/min. The air feed into the reactor was made free from moisture and CO2 by passing through it CaO and KOH pellet drying towers. The catalytic experiment was carried out in steady state conditions and the reaction temperature was increased from room temperature to 200oC with a heating rate of …show more content…
For controlling the heating temperature of the catalyst presence in a reactor is done by a micro-processor based temperature controller. The gaseous products are produced after the oxidation reaction in a reactor is analysis by an online gas chromatogram (Nucon series 5765) equipped with a porapack q-column, FID detector and a methaniser for measuring of the concentration of CO and CO2. The oxidation of CO at any instant was calculated on the basis of concentration CO in the feed and product stream by the following equations: (XCO) = [(CCO)in - (CCO)out ] / [CCO]in = [(ACO)in - (ACO)out ] / [ACO]in --------------- (2) Where, the concentration of CO is proportional to the area of chromatogram ACO. The overall concentration of CO in the inlet stream is proportional to the area of CO2 chromatogram. 3. Results and discussions The characterization of the different types of nitrate precursors prepared catalyst is done by following techniques and the activity of the catalyst for CO oxidation was discussed below. 3.1 Catalyst characterization The characterization of the catalyst is provide information about the morphology, surface area, binding energy, pore size, pore volume, chemical state, material composition and the percentages of different materials presence in a catalyst. 3.1.1 Scanning electron microscopy
Ernie Banks was one of the best baseball players in the MLB. He set many records for the Chicago Cubs. Ernie was one of the best Chicago has ever had. Being an athlete since birth, it was not hard to believe that his stats were the best in the majors. Ernie also showed his dedication by staying with the Cubs until his death.
Barbeque, fried chicken, trucks and farms. What comes to the minds of many after hearing such words is the southern portion of the United States. According to Judge Paul Health Till of Sidney, Texas other words that bring to his attention the culture of the South are manners, morals, customs and public opinions. Why so? In his essay Manners, Morals, Customs, and Public Perception (July 2001), Judge Till states “Manners and morals and customs make up the public perception of any culture” (paragraph two) and how these four key ideas relate to each other.
There are things that can be grouped as ‘unnecessary’ in this world, and The Story of Tom Brennan by J.C. Burke definitely falls into that category. Despite the fact that this book is targeted at teenagers, not all of them seem to enjoy reading the book. This is because first of all, many of them could not relate to any of the characters and secondly, Burke over-dragged a number of scenes. These made the novel ineffective and surely did not help the readers to enjoy reading. Tom Brennan is a 17 year-old rugby player and is a member of a family that was once respected in the town of Mumbili.
Not knowing anything about the history of railroads, can give one mixed feelings about diving into a reading like this. How is one going to feel, is one going to enjoy it, are some of the many questions that float around in the mind of the reader. The answers to these questions solely depend on the author and what they do to utilize their skills to try and convince or create feelings between the reading and reader. “Railroaded” by Richard White, was a book that was found to be very interesting and really opens eyes to see different views and perspectives on railroads. One can see the advancement of the nation, as only a positive in allowing us to move in a forward direction to better one’s life and future.
Tom murphy and John Colter both crossed Yellowstone in December. They both went alone with little supplies to explore Yellowstone, but Tom crossed what he knows is Yellowstone almost 200 years later than John, when Yellowstone park didn’t exist. Tom is only doing it for fun and excitement, where John did it to explore. He has a lot more gear that is a lot more advanced unlike John, who probably only had a coat, hat, glove, boots, and maybe a sleeping bag. People know the route Tom took but, no one really knows the route John took.
Fans of Deadliest Catch were shocked to hear that Jake Harris was attacked this week and left on the side of the road. His brother Josh Harris has been doing a great job of updating fans on how he is doing and what is going on. Jake ended up in ICU, and his brother Josh Harris kept going to his Facebook page to talk about what went down. He was worried about his brother and shared that they knew who attacked Jake. He even went as far as to share pictures of them and their names.
Born in San Francisco, California, Tim Hawkinson, 55, is a sculptural artist who currently works and resides in Los Angeles, California. Interestingly, there exists no single medium in particular that Tim employs in his works; rather, with a widely diverse variety of found, purchased, or created materials and components, each creation he builds is its own unique statement, each one a separate experiment in material study and fabrication. There are, however, several common themes that run through the majority of his pieces, in addition to the splash of flavor that is his own unique style and artistic methods. Often, Tim’s works are somewhat anatomical in nature; that is, a reflection of not simply the human body but also the essence of human
After watching the films of “Emmett Till and 4 Little Girl” I can see the parallels of history repeating itself with the murders of young black children. When we look at history, we are supposed to learn from our past mistakes as a society but unfortunately, some have not learned. We have once again witnessed the murders of young black children at the hands of white supremacy with not an ounce of justice for them or their families. None of these children did anything to deserve to die or become victims of such senseless murders. The saddest part apart the stories of Emmett Till and the four young ladies is that their bodies were all disfigured tot eh point the families had to use different identifies to figure out their bodies.
As a class requirement, we were obligated to watch a documentary about Emmett Till. The documentary, titled “The Murder of Emmett Till” was a tell-all about a tragic story of a fourteen-year-old boy from Chicago. Emmett Till was sent to Money, Mississippi to spend the summer with some relatives. In the 1950s, life in Chicago was different than life in Mississippi. Racism was stronger in the south than in the north and Emmett Till was walking into an environment he had never encountered before.
Comics are for Learners The graphic essay ,”Show and Tell” by Scott McCloud was written to prove that Graphic novels can be a useful tool to communication and that we see this form of communication through many mediums. To convey this message, McCloud uses classification and division to categorize all of his knowledge into concise and easy- to- understand categories for the reader. This theme of the usefulness of graphic novels is also seen in other works of McCloud, including his TED talk, describing his life, and his own official website, scottmccloud.com. McCloud’s views of graphic novels are used to show the reader and others that they are in fact a good source of knowledge;he believes that graphic novels can academically benefit students
A spin vane was added and a water-jacked condenser was attached. Isopentyl nitrite (0.06ml, 0.045 mmol) was dissolved in 1,2-dimethoxyethane (0.50 ml) in a 3-ml conical vial and caped to prevent loss by evaporation. Running the reaction. The mixture in the 5-ml conical vial containing the tetraphenylcyclopentadienone and anthranilic acid was heated on an aluminum block to 140° C. Once the mixture started to boil the prepared mixture of isopentyl nitrite was added to the 5-ml conical vial through the top of the condenser using a pasture pipette.
It was 1965 and Evel Knievel had just landed a 90-foot crate filled with 50 rattlesnakes and 2 lions. Although this jump was one of his stunts that left him unharmed other than a sprained ankle, it put others at risk. During his landing, the back tire of his motorcycle had hit the edge of box and allowed some of the snakes to escape. The audience that was watching Knievel’s stunt were terrified and had to run away in order to avoid the snakes. Despite knowing the risks of this stunt, he continued with it anyway.
Abstract: The purpose of this experiment was to identify given Unknown White Compound by conducting various test and learning how to use lab techniques. Tests that are used during this experiment were a flame test, ion test, pH test, and conductivity test. The results drawn from these tests confirmed the identity of the Unknown White Compound to be sodium acetate (NaC2H3O2) because there were no presence of ions and sodium has a strong persistent orange color. The compound then will be synthesized with the compounds Na2CO3 and HC2H3O2 to find percent yield.
Balanced Chemical Equation: Cu(s) + 4HNO3(aq) —> Cu(NO3)2 (aq) + 2NO2 (g) + 2H2O (l) Reaction 2: when sodium hydroxide (NaOH) is added to copper (II) nitrate (Cu(NO3)2), a double displacement reaction will occur. Copper and sodium will displace each other to create copper (II) hydroxide and sodium nitrate. Balanced Chemical Equation: Cu(NO3)2 (aq) + 2NaOH (aq) —> CuOH2 (s) + 2NaNO3 (aq) Reaction 3: When copper (II) hydroxide is heated, a decomposition reaction will occur. The reaction will decompose forming two compounds, Copper (II) oxide, and water. Balanced Chemical Equation: Cu(OH)2 (s) + Heat —> CuO (s)
Goerge Benson is an American musician who was born on the 22 of March 1943. He was an avid jazz musician and began his career as a jazz guitarist at the age of 21. He used a rest-stroke picking technique and loved scat singing and this can clearly be heard in the song. A rest-stroke picking picking technique is when one string on the guitar is picked and is followed through with strum of the following notes He was born and raised in Pennsylvainia, where he started out at the very bottom. As a young boy he played in bars and nightclubs illegally but he says his music always kept him on the straight and narrow and he is admired by many for his strong drive, motivation and willingness to put in the effort to make himself big and his name heard.