In this lab, three unknown compounds were separated from a mixture and identified by melting point. Unknown mixture #124 has components of acid, base and neutral compound. The compounds were identified by melting point and matched up with the known melting points from a given list. In order to identify the compound it was important to separate by dissolving the mixture in an organic solvent which was not soluble in water, and then extracting the solution first with HCl, and then dilute sodium hydroxide solution. From the separation mixture, the aqueous layer were obtained and labeled as TT-1 (base), TT-2(acid) and TT-3 (neutral) in three different test tubes for later recovery. The procedure steps were followed as indicated which led to the correct identification of the tree compounds. The experimental melting points of acid and base were fairly close to the theoretical melting point. However the melting points of neutral were not as close due to some impurities in the compound. Determination of melting point for sample #124 acid and base were accurate due to no presence of impurities. The base was correctly identified as 5-chloro-2- methoxyaniline with a …show more content…
More specifically, this lab was met in terms of gaining an understanding in separating an acid, base and neutral compound from a mixture and identify through melting point. Overall, the experiment was successful as the acid (benzoic), base (5-chloro-2- methoxyaniline) and neutral (biphenyl) compounds were correctly identified. The separation of mixtures compounds to give pure components is of great importance in chemistry and in specific in organic chemistry. Many synthetic reactions give mixtures of products and it is important to isolate the wanted compound with a precise methodology of extraction and purification. Identification of the compound can always be identified by melting point
The goal of this experiment was to isolate three different molecules (acidic, basic, and neutral) from a mixture and identify their molecular structure. This was accomplished by using acid/base liquid extraction and H NMR analysis. The neutral component of the unknown mixture #191 was fluorenone. This was evident due to an H NMR spectra that had a high presence of hydrogen signals in the 7.2- 7.7 ppm range. Chemical shift values for fluorenone stated in the lab manual were 7.27, 7.47, 7.48, and 7.6 (CITE), indicating that the corresponding H NMR spectra for the neutral unknown is of this chemical.
The purpose of this lab was to be able to use physical characteristics to determine the identity of an unknown compound. The data from this experiment classified aluminum as metallic; ascorbic acid, paraffin, palmitic acid, sucrose, graphite, and water as molecular; sodium chloride as ionic. In order to determine this, 3 tests were conducted. The first test was to test the conductivity of each substance at room temperature. In this test, only graphite and aluminum conducted.
To begin, the solubility of the unknown compound in water was tested. If the compound is soluble in water, it can be inferred that it is either a polar covalent or ionic compound.
Goals The primary goal of this experiment was to identify an unknown compound by running various tests to determine the qualitative solubility, conductivity, and pH value of the compound. Tests were also performed for the presence of specific cations and anions in the compound. The second goal was to discover the reactivity of the unknown compound by reacting it with different types of substances. The third goal of this project was to calculate the quantitative solubility of the unknown compound in water.
The boiling point range of Unknown 30A was 65.0 °C-67.2 °C. The two degrees difference in the boiling point range indicated that there were very few impurities presented in the liquid. The theoretically possible identities of the unknown were primary amines that contained higher boiling points than the range because of the higher altitude lab. However, sec-butylamine, with a boiling point of 63 °C, was included as a possible identities because it was only two degrees off of the range. Therefore, it was too early on in the experiment to eliminate a potential identity that was very close to the range.
Physically, the unknown compound was composed of white, grainy, crystal-like structures. The unknown was also odorless. From these observations, various physical and chemical testing was performed to determine properties of the unidentified compound. A series of solubility tests were performed, as shown in Table 2, and revealed that the unknown compound was soluble in water, but not in Acetone or Toluene.
Hence in the sample only copper (II) chloride will dissolve leaving the sodium chloride behind once filtered through. The copper (II) chloride can then be obtained by evaporating the methanol; which has a boiling point of 65 degrees celsius whilst copper (II) chloride has a boiling point of 993 degrees celsius, thus allowing the methanol to be easily evaporated out of the solution eliminating concerns of the copper (II) chloride evaporating alongside the methanol. Purpose To investigate different methods of separating copper (II) chloride and sodium chloride in order to obtain the original masses of both substances.
After obtaining an homogeneous mixture, the flask was placed in an ice bath during five minutes next to a graduated cylinder containing 5.0 mL of concentrated sulfuric acid. The temperature of the ice bath was recorded to be 1.1 °C. Likewise, a second graduated cylinder containing 1.8 mL of nitric acid and 2.5 mL of sulfuric acid was immersed in the cold ice bath to keep the three different solutions at the same temperature. Thereafter, the cold 5.0 mL of H2SO4 were added to the erlenmeyer flask containing the acetanilide solution, which remained in the cold water for approximately another 4 minutes.
In this lab, we tested 8 known ingredients to find what ingredients was in our unknown A and unknown B medications. We first tested the water solubility of our knowns and unknowns. We found that of the knowns, cornstarch and acetaminophen were the only ones not water soluble. The unknowns were also not water soluble. Th next test was the pH test.
Abstract: The purpose of this experiment was to identify given Unknown White Compound by conducting various test and learning how to use lab techniques. Tests that are used during this experiment were a flame test, ion test, pH test, and conductivity test. The results drawn from these tests confirmed the identity of the Unknown White Compound to be sodium acetate (NaC2H3O2) because there were no presence of ions and sodium has a strong persistent orange color. The compound then will be synthesized with the compounds Na2CO3 and HC2H3O2 to find percent yield.
TLC was used to identify the actual unknown product as well as other products/reactants present in the filtered solution. The procedure was conducted by placing a TLC plate in a developing chamber that is filled with a small amount of solvent. The solvent cannot be too polar because it will cause spotted compounds on the TLC plate to rise up too fast, while a very non-polar solvent will not allow the spots to move. The polarity of the spots also determines how far it moves on the plate; non-polar spots are higher than polar ones. After spots on the TLC form, the Rf values are calculated and used to analyze the similarity of the compounds.
Purpose/Introduction The process of recrystallization is an important method of purifying a solid organic substance using a hot solution as a solvent. This method will allow the separation of impurities. We will analyze Benzoic Acid as it is dissolved and recrystallized in water and in a solvent of Methanol and water. Reaction/Summary
Introduction: In this lab, of water in a hydrate, or a substance whose crystalline structure is bound to water molecules by weak bonds, is determined by heating up a small sample of it. By heating, the water of hydration, or bound water, is removed, leaving only what is called an anhydrous compound. Based on the percent water in the hydrate, it can be classified as one of three types: BaCl2O ⋅ 2H20, with a percent water of about 14.57%, CuSO4
Experiment #7: Column Chromatography of Food Dye Arianne Jan D. Tuozo Mr. Carlos Edward B. Santos October 12, 2015 Abstract Column chromatography is the separation of mixture’s components through a column. Before proceeding with the column chromatography itself, a proper solvent system must be chosen among the different solvents. The green colored food dye is the mixture whose components are separated.
Abstract The unknown concentration of benzoic acid used when titrated with standardized 0.1031M NaOH and the solubility was calculated at two different temperatures (20◦C and 30◦C). With the aid of the Van’t Hoff equation, the enthalpy of solution of benzoic acid at those temperatures was determined as 10.82 KJ. This compares well with the value of 10.27KJ found in the literature.