Benzaldehyde Essays

Purpose/Introduction The process of recrystallization is an important method of purifying a solid organic substance using a hot solution as a solvent. This method will allow the separation of impurities. We will analyze Benzoic Acid as it is dissolved and recrystallized in water and in a solvent of Methanol and water. Reaction/Summary In Experiment One we will be recrystallizing Benzoic Acid from water. In Experiment Two we will be recrystallizing Benzoic Acid using a solvent pair made up of Methanol

Initially, the conversion of benzyl alcohol in to benzaldehyde was chosen as a model reaction to optimize the reaction conditions. Effect of reaction time and mmol of H2O2 on progress of oxidation reaction was studied (Fig. 4. the experiment was performed with 20 mg catalyst, 10 ml acetonitrile and two different amount of H2O2 1 and 2 mmol for 1mmol benzyl alcohol at reflux condition (85 ºC ) and plotted with respect to the time. With increasing the mole ratio of BzOH : H2O2 from 1:1 to 1:2, the

Introduction: Benzaldehyde and acetone in ethanol solvent undergoes cross aldol condensation reaction to give dibenzalacetone. This reaction known as the Claisen-Schmidt reaction. Reaction: The benzalacetone, formed as an intermediate. Benzalacetone once formed, then easily react with another molecule of benzaldehyde to give dibenzalacetone. Procedure: 1. Take 8 mL of benzaldehyde in 100 mL beaker. 2. Add 2 mL of acetone to the benzaldehyde and mix. 3. Dissolve 5 g of NaOH into 50

reagents or compounds to each of the samples and then the mixture was observed for a reaction. The oxidation test, and 2,4-DNPJ test confirms that formaldehyde and benzaldehyde

Week 1 a simple condensation reaction between benzaldeyde and hydroxylamine produced the product benzaldehyde oxime that was found to be in oil. The percentage yield of the experiment is 64%. The 36% loss can be due to the solution needing to be neutralised with glacial acid, there was no way to tell if the reaction was neutralised, to help increase yield the use of pH indictor paper to indicate whether the reaction was neutralised. As by using a rotary evaporator to remove the organic solvent may

Sentwin India 5 NMR Bruker Advance II 400MHz 7 Heating Mantle Inco 6 Structure builder Chem draw Ultra 8.0 4.2 Experimental work: 4.2.1 General procedure for Chalcones: 2’-hydroxy acetophenone or 2’-hydroxy propiophenone (0.2ml) and substituted benzaldehydes (0.5 g) were mixed in the round bottom flask. After that 40% NaOH solution (4g NaOH in 10 ml of distilled water) and ethanol were added in round bottom flask. The reaction mixture was stirred upto 6-48 hours. Completion of reaction was monitored

To go in more depth, 98.2% is a high yield, despite the inaccuracies due to time constraints, and the inability to the recrystallize the benzoic acid. As mentioned earlier, product might have been lost during the many filtration procedures in the experiment, as not all of the product was poured out from the flask, onto the filter. Since, recrystallization could not be done, the benzoic acid was immediately transferred onto the watch glass, and it is when transferring some product could have been

allows for a carbon=carbon double bond to form from where a C=O double bond used to be located. Creating additional C=C double bonds is valuable due to its use in synthesis. The Wittig reaction will allow the synthesis of Stilbene (E and Z) from a Benzaldehyde (Ketcha, 141). One purpose of a Wittig reaction is the formation of alkenes from aldehydes or ketones employing a carbo-phosphorous ylide, which is stabilized vie resonance to allow for the carbon bonded to phosphorus to be deprotonate from by

and some Cannizzaro products would form as well. Since benzaldehyde was not added until after the carbanion formation, the Cannizzaro reaction should not have happened. This is supported by the absence of a white precipitate, which would indicate Cannizzaro products. Also, the use of a graduated pipette is important to ensure precise measurements of reagents. According to Calculations 2 and 3, the amount of moles of acetone and benzaldehyde are very similar, and this could make determining the limiting

As mentioned earlier, the molar mass of benzaldehyde is 106.121g/mol, and the molar mass of benzoic acid is 122.12g/mol. With that in mind, to calculate the maximum possible mass of benzoic acid, which is the product of the experiment, Equation #2 must be used. Referencing from Table 1.1, the observed benzaldehyde mass is 5.02g, thus the plugging that into Equation #2, the calculation would be, (122.12 g⁄mol C_7 H_6 O_2)/(106.121 g⁄mol C_7 H_6 O)×5.02g, equaling to, 5.78g±0.01g of benzoic acid.

between a Grignard reagent and an aldehyde leads to the production of a secondary alcohol. In fact, this is what we observed with regards to the experiment results. The addition reaction between the Grignard reagent, phenolmagnesium bromide, and benzaldehyde leads to the formation of diphenylmethanol, a secondary alcohol, as the product. As mentioned earlier, the reaction of the alkyl halide, bomobenzene, and magnesium metal turnings leads to the production of the Grignard reagent. This was observed

Synthesis of 3-[5-(4-substituted) phenyl-1,3,4-oxadiazole-2yl]-2-styrylquinazoline-4(3H)-ones was carried out by following steps: Step 1: Synthesis of 4- substituted benzaldehyde semicarbazon51(2) Semicarbazide Hydrochloride (0.1M) and sodium acetate (0.2M) was added and dissolved in 15-20ml of distilled water placed in flat-bottomed flask. In a separate beaker containing required aromatic aldehyde (1) (0.1M) was dissolved in aldehyde free alcohol. This ethanolic aromatic aldehyde solution was added

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reaction is only applicable to aromatic aldehyde and useful for the preparation of substituted cinnamic acid (Equation-3)[3] Equation-1 Equation-2 Equation-3 In 1883.A very important variation is done by plӧchl, which involve the heating of benzaldehyde

under the UV light the mixtures appeared a purple colour. The R_fValue Starting material: R_F=2.6/4.5 = 0.58 The sum: R_F=2.55/4.5 = 0.57 The reaction mixture: R_F=2.9/4.5 = 0.64 The final product: R_F=1.9/4.5 = 0.42 Table of calculations Benzaldehyde Acetone Sodium Hydroxide Ethanol Dibenzalacetone Co-efficient 2 1 1 1 1 Volume (ml) 4.04 1.5 30 Grams used (g) 4.2 1.185 4 0.95 2 Formula weight (g/mol) 106.12 58.08 40 46.07 234.29 Moles 0.0396 0.02 0.1 0.02 Moles/ Coefficient 0.02 0.02 0

3.3. Synthetic methodologies for dihydropyrimidinones 3.3.1. Classical method Scheme-1: The conventional method for the synthesis of DHPMs is the one-pot three-component reaction of benzaldehyde, ethyl acetoacetate and urea in the presence of an acid catalyst. The product of this novel one-pot, three components synthesis that precipitated on cooling of the reaction mixture was identified as 3,4-dihydropyrimidin-2(1H)-one and this reaction came to be known as “Biginelli reaction”, or “Biginelli condensation”

In his article, “Why McDonald Fries Taste So Good” Eric Scholosser takes a dive into the ingredients of the McDonald fries to uncover the secret behind the speed and taste of the fast food industry. Scholosser uses sensory images and pathos to inform the reader about the production secrets of many fast food restaurants. During his trip to the IFF(International Flavor & Fragrances), the largest flavor company in the world, Scholosser is asked to not take pictures inside of the factory. The factory

household liquids and growing rock candy, but I wanted to use the instruments and chemicals the professionals used. I wanted to be a real scientist. Never in my primitive years would I have imagined that I would be synthesizing aspirin and oxidizing benzaldehyde in high school. But as a student at Governor’ School at Innovation Park, I handle corrosive and carcinogenic

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Abstract: The main goal in our reaction was to use benzyl alcohol and (carbethoxymethylene)triphenylphosphorane along with a Wittig reagent to create ethyl cinnamate. Throughout the experiment, many observations were recorded that demonstrated the production of our product, including the production of a thick black substance. Synthesis steps were followed involving PCC and other reagents such as DCM to produce a 62.5% yield following the TLC and flash chromatography. IR and NMR were taken on the